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Wednesday, June 11th, 2008
10.00-15.00 Registration at Olympia terminal
11.00 Official opening
Ilkka Ojanperä, University of Helsinki, Helsinki, Finland
Workshops
11:30 Efficient use of the HPTLC approach
Colin Poole, Wayne State University, Detroit, USA
13:00-14:00 Lunch buffet at Buffet Symphony
14:00 Plant analysis in HPTLC: method development and validation
Eike Reich, CAMAG Laboratory, Switzerland
15:00 Validation for HPTLC: typical criteria and uncertainty
calculation according to CITAC Guide
Ingo Schellenberg, University of Applied Sciences Anhalt, Bernburg,
Germany
16:00-16:30 Coffee buffet at Congress department/Accommodation
17:00 Departure from Helsinki
Poster Session 1
16:30-17:30
News, fundamentals and theoretical aspects
Chairs: Imre Klebovitch and Heikki Vuorela
17:30 Quantitative micro planar chromatography – MPLC
Rudolf Kaiser, Institute for Chromatography, Bad Duerkheim, Germany
17:45 Pressurized planar electrochromatography – challenges and
perspectives
Tadeusz Dzido, Medical University, Lublin, Poland
18:00 Discussion
18:05 A comparative study of molecular lipophilicity indices of some formyland
acetylpyridine-3-thiosemicarbazone derivatives estimated by RPHPTLC
and calculated Log P values
Costel Sârbu, Babe-Bolyai University, Cluj-Napoca, Romania
18:20 The orthogonality of the selectivity space in reversed-phase thin-layer
chromatography
Colin Poole, Wayne State University, Detroit, MI, USA
18:35 Discussion
18:40 Ultrathin layer chromatography on plates with engineered nanostructure
Louis Bezuidenhout, University of Alberta, Edmonton, Canada
18:55 Fermentation monitoring based on HPTLC-OPLC technique: the effect
of a complex biological matrix on quantification performances
Tatiana Bernardi, University of Ferrara, Ferrara, Italy
19:10 Changes in emission induced by non-covalent analyte-fluorophore
interactions in silica gel as a general detection procedure for thin-layer
chromatography
Vicente Cebolla, CSIC, Zaragoza, Spain
19:25 Discussion
19:30 Welcome drink at Congress department
20:00 Buffet dinner at Buffet Symphony
Thursday, June 12th, 2008
09:30 Arrival in Stockholm
10:00-11:30 Sightseeing by bus
11:30-13:30 Freetime in old town/Takeaway lunch
Strong features of HPTLC
Chairs: Pierre Bernard-Savary and Gertrud Morlock
14:00 New test-kits to detect herbicide effects and resistance in weed plants
based on HPTLC-screening
Helle Weber Ravn, Aarhus University, Silkeborg, Denmark
14:15 Development of an HPTLC method for amino acid identification in
peptide
Roseline Sbaffo-Poasevara, IPSEN, Les Ulis, France
14:30 Discussion
14:40 HPTLC analysis of radioactive metabolites of 6-[18F]FDOPA after
modulation by enzyme inhibitors
Sarita Forsback, University of Turku, Turku, Finland
14:55 Complementarity of TLC and HPLC in investigation of triterpenoids in
plant extracts
Irena Vovk, National Institute of Chemistry, Ljubljana, Slovenia
15:10 Discussion
15:20 HPTLC for the analysis of API-cleaning samples
Ties Raijmakers, Organon (Schering-Plough Corporation), Oss, The
Netherlands
15:35 Is there a fine future for HPTLC in modern API plants?, Actual
experiences
Louise Vicard, Sanofi-Aventis, Neuville-sur-Saône, France
15:50 Discussion
16:00-16:40 Coffee buffet at Congress department
Specific applications
Chairs:Vicente Cebolla and Wolfgang Schwack
16:40 Determination of thiouracils in thin-layer chromatography with iodineazide
detection procedure
Robert Zakrzewski, University of Lódz, Lódz, Poland
16:55 Drug screening in autopsy liver samples by overpressured layer
chromatography
Anna Pelander, University of Helsinki, Helsinki, Finland
17:10 Discussion
17:20 Changes in glycoalkaloid composition during potato processing: simple
and reliable quality control via HPTLC
Jens Mäder, Berlin University of Technology, Berlin, Germany
17:35 A simple, accurate and rapid HPTLC method for the determination of
theophylline in post mortem blood and its validation
B. Mohan, Forensic Science Laboratory, Bangalore, India
17:50 Discussion
17:00 Departure from Stockholm
18:00-18:20 Break
Detection, bioactivity tests, and coupling techniques
Chairs: Tadeusz Dzido and Irena Vovk
18:20 A new method for the quantification of Quats by TLC
Bernd Spangenberg, University of Applied Sciences Offenburg,
Offenburg, Germany
18:35 A new multi-enzyme inhibititon test for the detection of insecticidal
organophosphates and carbamates by HPTLC
Wolfgang Schwack, University of Hohenheim, Stuttgart, Germany
18:50 Discussion
18:55 HPTLC/AMD with Vibrio fischeri as an example for bioactivity-based
detection - A new dimension in analytics
Wolfram Seitz, Zweckverband der Landeswasserversorgung,
Langenau, Germany
19:10 Advanced mass spectrometric approaches for the analysis of analytes
on planar separation media
Vilmos Kertesz, Oak Ridge National Laboratory, Oak Ridge, TN, USA
19:25 Discussion
19:30 Combined TLC-MALDI analysis of lipids
Jürgen Schiller, University of Leipzig, Leipzig, Germany
19:45 Automated coupling of planar chromatography with mass spectrometry
Gertrud Morlock, University of Hohenheim, Stuttgart, Germany
20:00 Discussion
21:00 Symposium dinner at Bistro Maxime
FRIDAY, 13th MAY
Poster Session 2
09:00-10:00
09:55 Arrival in Helsinki (check-out from cabins)
Manufacturers’ Session
Chairs: Louise Vicard and Tatiana Bernardi
10:00 Applications of HPTLC in the cGMP for dietary supplements
Eike Reich, Camag, Muttenz, Switzerland
10:20 HPTLC/DESI-MS for the analysis of proteins and peptides
Michael Schulz, Merck, Darmstadt, Germany
10:40 New Horizons in Instrumental TLC
Rolf Rolli, CAMAG, Muttenz, Switzerland
Poster Awards
Committee: Friedrich Geiss, Bernd Spangenberg and Ilkka Ojanperä
11:10-11:20 Poster awards
Closing Remarks
Colin Poole and Rudolf Kaiser
11:20 Closing remarks
11:30 Jubilee lecture
11:40 Farewell cocktail
12:00 End of Symposium
POSTERS LIST
Poster Session 1
Discussion time: Wednesday 16.30-17.30
Posters shown: Wednesday 10:00 – Thursday 14:00
General
1. Why HPTLC in the age of ultra-rapid HPLC separations?
Morlock Gertrud, University of Hohenheim, Stuttgart, Germany
2. Fast identification by HPTLC-MS on-line coupling
Carminati Alain, Sanofi Aventis, Process Development Chemistry, Sisteron,
France
Pharmaceutical and biomedical analysis
3. RP HPTLC investigation of some salicylic acid derivatives
Djaković-Sekulić Tatjana, Faculty of Sciences, Novi Sad, Serbia
4. Investigation of the lipophilicity of newly synthesized derivatives of secoandrostene
using RP-HPTLC. Biological activity
Djaković-Sekulić Tatjana, Faculty of Sciences, Novi Sad, Serbia
5. Applications of HPTLC as a problem solving technique in pharmaceutical
analysis
McKinlay Clare, GlaxoSmithKline, Stevenage, UK
6. Bile acids: separation and quantification by thin layer chromatography
Tavel Elisabeth, Sanofi-Aventis, Neuville sur Saône, France
7. TLC detection of Kryptofix 2.2.2 of [18F]FDG injections
Kirjavainen Anna, Turku PET Centre, Turku, Finland
8. Development of high performance thin layer chromatographic profile for ISM
drugs and their substitutes/adulterants
Saraswathy A., Captain Srinivasa Murti Drug Research Institute for Ayurveda
and Siddha, Chennai, India
9. Pharmacokinetic determination of ursolic acid in Alstonia scholaris R. Br. using
high performance thin-layer chromatography
Shetty Prabha, Sophia College, India
10. TLC densitometric determination of oxitetracycline
Simonovska Breda, National Institute of Chemistry, Ljubljana, Slovenia
11. Comparative studies on analyses of lipids by NH2-silica gel columns and
styrene – divinylbenzene from Supelco and Macherey-Nagel
Popa Iuliana, Laboratory of Dermatological Research, University of Lyon I,
Edouard Herriot Hospital, Lyon, France
12. Validated TLC-densitometric analysis for determination of carotenoids in
serum from Fancy Carp (Cyprinus carpio): Evaluated pharmacokinetic
parameters
Yangsoir Bundit, Department of Aquaculture, Faculty of Fisheries, Kasetsart
University, Bangkok, Thailand
13. Inhibition of cholinesterases by coumarin 106 as measured by a combination
of microtiter-well and TLC assays
Sandberg Malena, Department of Biochemistry and Pharmacy, Åbo Akademi
University, Turku, Finland
Environmental and forensic analysis
14. Application of iodine-azide reaction in thin-layer chromatography for the
determination of metal dithiocarbamate
Zakrzewski Robert, University of Lódz, Lódz, Poland
15. Quantification of additives in mineral oil by HPTLC confirmed by mass
spectrometry and infrared spectroscopy
Dytkiewitz E., University of Hohenheim, Stuttgart, Germany
16. High performance thin-layer chromatography: application to the detection of
traces of explosives after attack
Gleize Joannès, Laboratoire central de la Préfecture de Police, Paris, France
17. Bio-activity based analysis of irradiated sunscreens using HPTLC and in situ
detection with Vibrio fischeri
Baumgartner Vera, State Laboratory of the Canton Basel City, Basel,
Switzerland
Poster Session 2
Discussion time: Friday 09:00-10.00
Posters shown: Thursday 14:00 – Friday 11:00
Herbal analysis
18. Different extraction techniques of flavonoid bioactive compounds from
Satureja hortensis L. and HPTLC analysis
Soran Maria-Loredana, National Institute of Research & Development for
Isotopic and Molecular Technology, Cluj-Napoca, Romania
19. HPTLC quantification of some flavonoids from Satureja hortensis L. extracts
obtained with different extraction techniques
Bros Ildiko, “Babes-Bolyai” University, Cluj-Napoca, Romania
20. Analysis of the essential oil of Satureja hortensis L. by HPTLC
Bros Ildiko, National Institute of Research & Development for Isotopic and
Molecular Technology, Cluj-Napoca, Romania
21. Simple TLC-densitometric analysis of plaunotol for screening of high-plaunotol
containing plants of Croton stellatopilosus Ohba
Rinthong Prasob-orn, Chulalongkorn University, Bangkok, Thailand
22. Characterization and purification of proanthocyanidins from cranberry fruits by
modern planar chromatography (TLC, AMD, OPLC)
Pothier Jacques, Laboratoire de Pharmacognosie, Univ. Tours, Tours,
France
23. Characterization of some flavonosides from Poaceae by HPTLC and OPLC
Pothier Jacques, Laboratoire de Pharmacognosie, Univ. Tours, Tours,
France
24. When TLC helps the botanist to identify suspect samples
Pothier Jacques, Laboratoire de Pharmacognosie, Univ. Tours, Tours,
France
25. Improvement of thin layer chromatography for enzyme assay of
geranylgeraniol 18-hydroxylase from Croton stellatopilosus Ohba
Wunnakup Thaniya, Chulalongkorn University, Bangkok, Thailand
Food analysis
26. New HPTLC/FLD method for analysis of dialkyl phosphates as breakdown
products of organophosphorus insecticides during fruit juice processing
Schwack Wolfgang, University of Hohenheim, Stuttgart, Germany
27. Determination of histamine with TLC-densitometry in fish and fishery products
Bajc Zlatka, Veterinary Faculty, Ljubljana, Slovenia
28. Metabolism of 14C-IR6141 in grapes, lettuce and tomato
Garau Stefano, Isagro Ricerca Srl, Novara, Italy
29. Rapid analysis of sucralose in various food matrices
Morlock Gertrud, University of Hohenheim, Stuttgart, Germany
30. Rapid SBSE-HPTLC/FLD method for quantification of polycyclic aromatic
hydrocarbons (PAH) in drinking water
Morlock Gertrud, University of Hohenheim, Stuttgart, Germany
31. Method comparison for quantification of heterocyclic aromatic amines in fried
meat
Morlock Gertrud, University of Hohenheim, Stuttgart, Germany
32. HPTLC determination of epicatechin and procyanidin B2 in chocolate samples
after matrix solid-phase dispersion
Mutavdžić Pavlović Dragana, Faculty of Chemical Engineering and
Technology, Department of Analytical Chemistry, Zagreb, Croatia
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